The Synthesis and Characterization of Tribophysical Layers on Diamond and Silicon Carbide Surfaces

Abstract

A new ultrahigh vacuum apparatus, dedicated to the study of the surface chemistry of diamond single crystals, has been completed and the first scientific experiments have been done. This apparatus incorporates XPS, LEED, ESDIAD, HREELS, and TPD facilities for the study of the fluorination and hydrogenation of diamond single crystals. The apparatus is being employed for studies of atomic hydrogen/deuterium adsorption on diamond(100) in initial experiments prior to the use of XeF2 as a fluorinating agent. It is proposed to study the formation of CHx and CFx surface species, the thermal desorption products from these species, the resistance to oxidation by these species, and the functionalization of the diamond surface by fluorinated molecules such as C2F4, NF3, and CF3CF. Collaborative AFM studies of diamond AFM tips sliding over our diamond(100) single crystal are underway, in work being done with Dr. Gary McClelland at IBM Almaden. Frictional studies completed on the non-modified surface will be compared to studies on fluorinated diamond(100).

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1992
Accession Number
ADA250983

Entities

People

  • John Yates

Organizations

  • University of Pittsburgh

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Adsorption
  • Charge Carriers
  • Chemistry
  • Desorption
  • Deuterium
  • Electron Beams
  • Fluorination
  • Heat Energy
  • Hydrogen
  • Hydrogenation
  • Mass Spectrometers
  • Measurement
  • Single Crystals
  • Spectra
  • Surface Chemistry
  • Vacuum
  • Vacuum Apparatus

Fields of Study

  • Physics

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Organic Chemistry
  • Thin Film Deposition Science.