Substituent Effects and Bonding Characteristics in o- Benzoquinonediiminebis(bipyrdine) Ruthenium(II) Complexes

Abstract

The effect of substituents on the electrochemistry and electronic spectroscopy of RuII(bpy)2LL complexes is reported, where bpy = 2,2'-bipyridine and LL = 4,5-disubstituted o-benzoquinonediimines, o-semiquinonediimines, o- phenylenediamides and o-phenylenediamines. These data are used to create a map of the orbital energies as a function of the Hammett parameter of the substituents, giving insight into the electronic behavior of these complexes. Electronic spectra are characterized with respect to energy, intensity and bandwidth, and bands are assigned with support from resonance Raman (rR) and FTIR data. The solvatochromism Of the o-benzoquinonediimine species is discussed. The data are interpreted in the context of metal-ligand orbital mixing and electronic structure. An ab initio study of the uncomplexed ligand in its quinonediimine oxidation state, is also included. Ruthenium, Electrochemistry, Quinone, Benzoquinonediimine, Electronic Spectra.

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Document Details

Document Type
Technical Report
Publication Date
Oct 23, 1992
Accession Number
ADA257346

Entities

People

  • Alfred Beverley Philip Lever
  • E. S. Dodsworth
  • H. Masui

Organizations

  • University of York

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  • Energy and Power Technologies

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  • Bandwidth
  • Carbonate Esters
  • Chemical Analysis
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Electrochemistry
  • Inorganic Chemistry
  • Materials Science
  • Mixing
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  • New England
  • North Carolina
  • Organic Chemistry
  • Raman Spectra
  • Spectra
  • United States

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  • Chemistry

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