The Design and Construction of an Ion Trap Based System for Laser Pyrolysis/Mass Spectrometry of Single Organic Aerosol Particles

Abstract

This report describes the development of particle introduction techniques to support a 3 year program for analysis of single bacteria via laser pyrolysis/mass spectrometry. Results of an investigation into various sample introduction techniques are discussed including the highly successful quasi- electrospray introduction method using a suspension of particles in methanol. Particles from .9 to 13 um have been levitated at pressures down to 10-7 torr, and mass spectrometry pressures of 10-3 torr have been obtained in less than 10 min from particle. The effectiveness of these techniques for particle introduction, pump down and stabilization has exceeded of the authors expectations and gives a positive prognosis for efforts to perform initial laser pyrolysis/mass spectrometry experiments in the year 2 effort.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Oct 01, 1992
Accession Number
ADA260455

Entities

People

  • George Hars
  • Henk L. Meuzelaar
  • Neil S. Arnold
  • Paul A. Cole

Organizations

  • University of Utah

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Alcohols
  • Bacteria
  • Barometric Pressure
  • Chemistry
  • Dissociation
  • Electrospray
  • High Vacuum
  • High Voltage
  • Ion Traps
  • Mass Spectra
  • Mass Spectrometry
  • Methanols
  • Particle Size
  • Particles
  • Pyrolysis
  • Spectrometry
  • Trajectories

Readers

  • Aerosol Science/Aerosol Physics
  • Optical Physics and Photonics.
  • Systems Analysis and Design

Technology Areas

  • Directed Energy