Applications of Low-Coordination Phosphorus Chemistry in the Chemical Modification of Surfaces

Abstract

Low-coordination phosphorus compounds of various types (RO-PO2, R-PO2, RO-P(S)O, R-P=CH2) were generated in the presence of suspended solids known to contain surface OH groups (silica gel, alumina, Zeolites, titanium dioxide). In all cases, the phosphorus atom became covalently attached to the 0 atom on the surface. CP-MAS 31P NMR was used extensively to prove the presence of the bonded group. Valuable HPLC characteristics were found for phosphorylated silica gel.

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Document Details

Document Type
Technical Report
Publication Date
Nov 13, 1992
Accession Number
ADA261208

Entities

People

  • Louis D. Quin

Organizations

  • University of Massachusetts Amherst

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Alkenes
  • Chemical Synthesis
  • Chemistry
  • Chlorides
  • Mass Spectrometry
  • Materials
  • Organic Chemistry
  • Organophosphorus Compounds
  • Oxides
  • Petroleum
  • Phosphorus
  • Phosphorus Compounds
  • Silica Gels
  • Spectra
  • Spectroscopy

Readers

  • Molecular and Cellular Biochemistry
  • Organic Chemistry
  • Surface Coatings Technology.