13 C NMR Spectra of Allosteric Effectors of Hemoglobin

Abstract

In the last three years many papers dealing with the preparation and biological activity of compounds that act as allosteric effectors of hemoglobin have been published. Among the numerous moieties, some urea derivatives were found to be very effective in reducing oxygen affinity of hemoglobin. The structures of most of the compounds were confirmed by 1H NMR spectra; however, to our knowledge, 13C NMR spectra have not been published for any of these allosteric modifiers of hemoglobin. We prepared in this series over 30 new urea and thiourea derivatives with the intent of investigating their biological activity. An analysis of 13C NMR spectra revealed high regularity in the chemical shifts of the similar fragments of the structures and revealed signal deviations among structures having different substituents in the aromatic rings.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1993
Accession Number
ADA262979

Entities

People

  • Stanislaw Ostrowski
  • Thomas G. Burke
  • Waldemar Priebe

Organizations

  • Ohio State University

Tags

DTIC Thesaurus Topics

  • Acquisition
  • Chemical Shifts
  • Couplings
  • Experimental Data
  • Fluorine
  • Hemoglobin
  • Measurement
  • Melting Point
  • Military Research
  • Plastic Explosives
  • Spectra
  • Spectrometers
  • Two Dimensional
  • Universities

Fields of Study

  • Chemistry

Readers

  • Molecular and Cellular Biochemistry
  • Organic Chemistry
  • Theoretical Analysis.