Properties of Superconducting YBa2Cu3O6+4 Ceramic Materials: Effect of Processing Parameters

Abstract

The effect of the sintering temperature, the sintering time and the addition of 5 wt. % silver on the average particle size, bulk density and the superconducting zero resistance temperature (Tc) YBa2CU306+x ceramic materials was investigated (a) in the range 880 - 940 deg C for 2 hours and (b) at 920 deg C for different times in the range 0-10 hours. The results suggest that while the density and particle size of the sintered ceramic increases with an increase of the sintering temperature (and 2 hours of sintering), prolonged sintering (at 9200C) above 4 hours of duration does not improve above properties. However, the superconducting zero resistance temperature (Tc) does not change significantly. In the presence of 5 wt. % silver, it appears that both sintering temperature and duration of sintering significantly improves the bulk density, particle size and (Tc) of YBa2CU30r6+x.... Morphology, Superconductivity, Sintering, Temperature, Time.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 1993
Accession Number
ADA263441

Entities

People

  • A. S. Rao

Organizations

  • Naval Surface Warfare Center Carderock Division

Tags

DTIC Thesaurus Topics

  • Ceramic Materials
  • Chemical Reactions
  • Composite Materials
  • Crystal Structure
  • Electrical Properties
  • Electrical Resistance
  • Fabrication
  • Grain Boundaries
  • Grain Growth
  • Grain Size
  • High Temperature
  • Materials
  • Materials Processing
  • Microstructure
  • Particle Size
  • Particles
  • Resistance

Fields of Study

  • Materials science
  • Physics

Readers

  • Superconducting Magnet Technology
  • Surface Engineering/Surface Coating Technology.