Electrode Potential-Induced Reconstruction of Au(100): Effect of Chemisorption of Nanoscale Dynamics as Probed by In-Situ Scanning Tunneling Microscopy

Abstract

The effect of iodide chemisorption on the nanoscale real-space dynamics associated with the electrode potential-induced formation and removal of the hexagonal reconstruction on Au(100) in aqueous solution has been examined by means of in-situ scanning tunneling microscopy under potentiodynamic conditions. Unlike in 'non-adsorbing' media such as perchloric acid where the (1 x 1) yields (hex) phase change is slow (T 1/2 approx. 10 min), requiring adatom diffusion from terrace edges, the potential-induced transition in iodide can be remarkably rapid (< 0.2 s). The latter features facile large-scale (ca 10-20 nm) gold mass transport emanating from former (1 x 1) terraces as well as from terrace edges. The likely roles of chemisorption in inducing such remarkably rapid reconstruction are briefly discussed.

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1993
Accession Number
ADA265900

Entities

People

  • Michael J. Weaver
  • Xiaoping Gao

Organizations

  • Purdue University

Tags

DTIC Thesaurus Topics

  • Acids
  • Adsorption
  • Chemisorption
  • Chemistry
  • Crystal Lattices
  • Diffusion
  • Dynamics
  • Electrodes
  • Electrolytes
  • Mass
  • Mass Flow
  • Metals
  • Perchloric Acid
  • Phase
  • Phase Transformations
  • Physical Chemistry
  • Transitions

Fields of Study

  • Physics

Readers

  • Electrochemical Surface Science
  • Thin Film Deposition Science.

Technology Areas

  • Space
  • Space - Hall-Effect Thruster