Large Odd-Numbered Carbon Clusters from Fullerene-Ozone Reactions

Abstract

The odd-numbered carbon clusters C119, C129 and C139 have been observed in the mass spectra of toluene extracts of fullerene soots and of the products of ozone-fullerene reactions. Specifically, ozone-C60 reactions yield C119, and ozone-C70 reactions yield C139, and ozone-(C60/C70) reactions produce C119, C129, and C139. These unexpected species correspond to dimers of C60, C60/ C70, and C70, respectively, less one carbon atom, and are stable gas-phase ions with behavior similar to that of fullerenes. The results suggest a new route to functionalization and derivatization of fullerenes through controlled ozone- catalyzed cage-opening reactions.

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Document Details

Document Type
Technical Report
Publication Date
Jun 11, 1993
Accession Number
ADA268633

Entities

People

  • Donald R. Huffman
  • John H. Callahan
  • Lowell D. Lamb
  • Mark M. Ross
  • Stephen W. Mcelvany

Organizations

  • United States Naval Research Laboratory

Tags

Communities of Interest

  • Energy and Power Technologies
  • Materials and Manufacturing Processes
  • Weapons Technologies

DTIC Thesaurus Topics

  • Abstracts
  • Chemical Reactions
  • Chemistry
  • Desorption
  • Fullerenes
  • Ionization
  • Mass Spectra
  • Mass Spectrometers
  • Mass Spectrometry
  • Military Research
  • Radiation
  • Reaction Mechanisms
  • Spectra
  • Spectrometers
  • Spectrometry
  • Surface Warfare
  • Ultraviolet Radiation

Fields of Study

  • Chemistry
  • Environmental science

Readers

  • Organic Chemistry
  • Quantum Chemistry