Dense Energetic Compounds of C, H, N, and O Atoms. III. 5-(4-Nitro-(1,2, 5)oxadiazolyl)-5H-(1,2,3)triazolo(4,5-c)(1,2,5)oxadiazole
Abstract
Diazidoazofurazan 8 was obtained from the bis-diazonium salt of diaminoazofurazan 7 by treatment with sodium azide and underwent thermolysis to 5-(4-azido-(1,2,5)oxadiazolyl)-5H-(1,2,3)triazolo(4,5,-c)(1,2,5)oxadiazole 5. The corresponding amine 13 was obtained from the azide 5 by reduction with stannous chloride and was oxidized by ammonium persulfate to 5-(4 nitro-(1,2,5) oxadiazolyl)-5H-(1,2,3)triazolo(4,5-c)(1,2,5)oxadiazole 1. The azide 5 was converted to a phosphinimine 9 in a reaction with triphenylphosphine
Document Details
- Document Type
- Technical Report
- Publication Date
- Jul 21, 1993
- Accession Number
- ADA268715
Entities
People
- Ananthakrishnan Gunasekaran
- Joseph H. Boyer
Organizations
- University of New Orleans