Synthesis and Characterization of Two-Dimensional Molecular Recognition Interfaces

Abstract

We have used self-assembly chemistry to synthesize monolayer assemblies that function as molecular recognition interfaces. In the first part of this paper, we show that one-component self-assembled n-alkanethiol monolayers with carboxylic acid functionalized endgroups specifically adsorb vapor-phase acid-terminated molecules via hydrogen bonding or vapor-phase amine- terminate molecules via proton-transfer interactions. In the second part, we demonstrate that two-component monolayers, which consist of inert n-alkanethiol framework molecules and--defect-inducing template molecules, can discriminate between solution-phase probe molecules based on their physical and chemical characteristics. By electrochemically etching the defects and then imaging the resulting surface by scanning tunneling microscopy the defect sites can be indirectly visualized.

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Document Details

Document Type
Technical Report
Publication Date
Nov 23, 1993
Accession Number
ADA273177

Entities

People

  • C. B. Ross
  • J. K. Schoer
  • Liuyang Sun
  • O. Chailapakul
  • R. M. Crooks

Organizations

  • University of New Mexico

Tags

Communities of Interest

  • Energy and Power Technologies
  • Engineered Resilient Systems
  • Sensors

DTIC Thesaurus Topics

  • Assembly
  • Carboxylic Acids
  • Chemical Synthesis
  • Chemistry
  • Films
  • Frequency Shift
  • Hydrogen
  • Manufacturing
  • Molecules
  • Monomolecular Films
  • Physical Properties
  • Recognition
  • Self Assembled Monolayers
  • Self Assembly
  • Small Molecules
  • Two Dimensional
  • Vapor Phases

Fields of Study

  • Chemistry

Readers

  • Nanocomposite Materials Science
  • Semiconductor Device Technology