Cryogenic Size Reduction of Solid Propellant

Abstract

A growing need exists to develop improved methods for the disposal and/or recovery of solid rocket propellants. Laboratory, bench-scale, and prototype tests were performed to develop the dry washout concept for size reduction and removal of solid propellants using cryogenic media. Three propellant types were investigated: Hazard Class 1.1 composite modified double base (CMDB), Hazard Class 1.1 cross-linked double base (XLDB), and Hazard Class 1.3 hydroxl terminated polybutadiene (HTPB). No propellant initiations were detected. The laboratory tests established that essentially no change in the sensitivity of the test propellants occurs between ambient and cryogenic temperature. Impact, friction, low-level shock and electrostatic discharge sensitivity tests were conducted. Over 2000 trials were conducted. The bench- scale tests demonstrated the safety of liquid nitrogen washout and established parameter ranges for effective propellant removal. Removal rates of greater than 60 pounds per hour were achieved for all propellant types. The prototype tests demonstrated cryogenic washout of several reduced scale motors in a semiautomated process. Two motors were processed, one containing 40 pounds of XLDB propellant, the other containing 60 pounds of HTPB propellant. Propellant removal rates ranged from 8.3 pounds per hour to 156 pounds per hour with liquid nitrogen flow of less than 4 gpm.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 1993
Accession Number
ADA274844

Entities

People

  • Michael H. Spritzer
  • Will P. Creedon

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Civil Engineering
  • Composite Propellants
  • Double Base Propellants
  • Electrical Properties
  • Energetic Materials
  • Explosives
  • Hydroxyl Terminated Polybutadiene
  • Laboratory Tests
  • Material Degradation Processes
  • Materials
  • Materials Laboratories
  • Materials Testing
  • Propellants
  • Rocket Propellants
  • Solid Propellants
  • Synthetic Rubber
  • Test Facilities

Fields of Study

  • Physics

Readers

  • Environmental Engineering.
  • Rocket Propulsion.