'Living' Radical Polymerization. 1. Possibilities and Limitations

Abstract

Possibility of the synthesis of well-defined polymers by radical polymerization is discussed. Kinetic analysis demonstrates that the preparation of polymers with controlled macromolecular structure in a 'living' radical process requires low stationary concentration of growing radicals which are in a dynamic equilibrium with dormant species. Three approaches are described. First, when growing radicals react reversibly with scavenging radicals to form covalent species, second when growing radicals react reversibly with covalent species to produce persistent radicals and the third in which growing radicals participate in the degenerative transfer reaction which regenerates the same type of radicals. Some of the reported 'living' radical systems are critically evaluated.

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Document Details

Document Type
Technical Report
Publication Date
Jun 30, 1994
Accession Number
ADA281042

Entities

People

  • Daniela Mardare
  • Dorota Greszta
  • Krzysztof Matyjaszewski

Organizations

  • Carnegie Mellon University

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Alkenes
  • Block Copolymers
  • Chemical Reactants
  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Free Radicals
  • Macromolecules
  • Molecular Weight
  • Organic Chemistry
  • Organometallic Compounds
  • Polymer Chemistry
  • Polymerization
  • Polymers
  • Side Reactions

Fields of Study

  • Chemistry

Readers

  • Combustion science or combustion engineering.
  • Economics
  • Nanocomposite Materials Science