X-Ray Absorption Spectra and Structure of Some Nickel Oxides (Hydroxides)

Abstract

The structure of the higher oxide forms of nickel (where Ni has a valency greater than +2) is of great interest from the standpoint of developing advanced nickel batteries for consumer applications and for electric vehicle propulsion. In spite of various research efforts, much uncertainty and confusion still exists with regard to the stoichiometry and structure of the various oxides (hydroxides) that are formed during the charging (and discharging) of the nickel electrode. The difficulty stems in part from the highly disordered or amorphous nature of the phases formed which makes structural determination by X- ray diffraction difficult. X-ray absorption fine structure (XAFS) spectroscopy is an excellent technique for the characterization of such materials which have no longer range order and can be used for in situ measurements.

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Document Details

Document Type
Technical Report
Publication Date
Jun 28, 1994
Accession Number
ADA281305

Entities

People

  • Azzam N. Mansour
  • C. A. Melendres

Organizations

  • Naval Surface Warfare Center

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Absorption
  • Absorption Spectra
  • Atomic Structure
  • Atoms
  • Chemistry
  • Diffraction
  • Electric Vehicles
  • Electrochemical Cells
  • Hydroxides
  • Inorganic Chemistry
  • Materials
  • Oxides
  • Spectra
  • Spectroscopy
  • Surface Warfare
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Physics

Readers

  • Materials Science and Engineering.
  • Surface Engineering/Surface Coating Technology.
  • Systems Analysis and Design