Well-Defined Polyphosphazenes by Anionic Polymerization of Phosphoranimines

Abstract

Polyphosphazenes form an important class of polymers with unique properties which include a combination of high temperature stability, low temperature flexibility, low surface energy, biofriendliness, inflammability, etc. The classic synthetic approach provides very high molecular weight polymers with broad polydispersities and with no control of end groups in low yields and under extreme conditions (a few days at temperatures above 200 deg C in a highly corrosive medium). The purpose of the project investigated in our laboratories was to develop alternative routes to polyphosphazenes. New synthesis should provide well defined polymers in higher yields and under milder conditions. Especially important is the control of structural features of polyphosphazenes including control of molecular weights, polydispersities, tacticities and terminal functionalities. We focused our research on catalyzed polymerization of phosphoranimines and synthesis of poly(diarylphosphazenes) via silyl azide intermediates.

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Document Details

Document Type
Technical Report
Publication Date
Jun 20, 1994
Accession Number
ADA281414

Entities

People

  • Krzysztof Matyjaszewski

Organizations

  • Carnegie Mellon University

Tags

Communities of Interest

  • Advanced Electronics
  • Human Systems

DTIC Thesaurus Topics

  • Block Copolymers
  • Chemistry
  • Copolymers
  • Electron Diffraction
  • Exchange Reactions
  • High Temperature
  • Low Temperature
  • Macromolecules
  • Materials
  • Military Research
  • Molecular Weight
  • Phosphine
  • Polymerization
  • Polymers
  • Scientists
  • Students
  • Surface Energy

Fields of Study

  • Chemistry

Readers

  • Polymer Science and Technology