NMR Studies of Polymers at Interfaces

Abstract

A review of NMR studies done in our laboratory on the dynamics of polymers adsorbed at interfaces is made. Of specific interest is polymers adsorbed on solid substrates at the (1) solution, (2) gas, and (3) polymer interface. In solution we have used deuterium NMR relaxation times to show the enhanced motional mobility of styrene segments of vinylpyridine-styrene block copolymers, adsorbed on silica, and swollen with toluene. At the gas interface, we show how the presence of the interface can turn a rubbery polymer into a glassy one with carbon-13 studies of poly(iso-propyl acrylate). At the polymer interface, we show how the overpolymerization of bismaleimide slows the dynamics of the interfacial layer of silane coupling agent. Polymers, Interfaces, NMR, Surfaces.

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Document Details

Document Type
Technical Report
Publication Date
Jul 08, 1994
Accession Number
ADA281570

Entities

People

  • Frank D. Blum

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Abstracts
  • Acrylates
  • Block Copolymers
  • Chemistry
  • Composite Materials
  • Copolymers
  • Couplings
  • Deuterium
  • Dynamics
  • Macromolecules
  • Materials
  • Materials Science
  • Mobility
  • Polymers
  • Relaxation Time
  • Substrates
  • United States

Fields of Study

  • Chemistry

Readers

  • Polymer Science and Engineering.
  • Quantum spin resonance or Electron Paramagnetic Resonance spectroscopy.
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics