AASERT-93: Electroplating of Refractory Metals Using Haloaluminate Melts

Abstract

The main objective of this research, performed by Sven E. Eklund, a graduate student at the Univ of Tennessee, Knoxville, is to explore the fundamentals of electroplating of several refractory metals, such as tungsten and tantalum, from chlorofluoroaluminate melts and to compare with electroplating of these elements from the LiF-NaF-KF eutectic. There has been considerable interest in the electrochemistry and metallurgy of the Groups IV-B, V-B, and VI-B4 transition metals (so-called refractory metals) because of the potential use of these metals in electronic components, electrical devices, and the aerospace industry. Pure, coherent deposits of these metals were originally obtained by a method developed by Mellors and Senderoff (1) in 1965. This method uses electrolytic reduction to the metal from the ternary eutectic LiF-NaF-KF, or FLINAK. Mechanisms proposed in several articles by Senderoff and coworkers for the reduction of several metals (2-5) have spurred research into the refractory metals in molten fluorides.

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Document Details

Document Type
Technical Report
Publication Date
Aug 31, 1994
Accession Number
ADA284859

Entities

People

  • Gleb Mamantov

Organizations

  • University of Tennessee system

Tags

DTIC Thesaurus Topics

  • Aerospace Industry
  • Air Pollution
  • Chemical Compounds
  • Chemistry
  • Electrochemistry
  • Electroplating
  • Elements
  • Fluorides
  • Low Temperature
  • Materials
  • Materials Science
  • Metals
  • Oxides
  • Refractory Metals
  • Tantalum
  • Transition Metals
  • Tungsten

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Microelectronics
  • Space
  • Space - Hall-Effect Thruster