Effects of Molecular Structure on the Electroactive and Optical Properties of Conjugated Rigid-Rod Polybenzobisazoles.

Abstract

The effects of molecular structure on the electronic structure and electrochemical and linear optical properties of a series of pi-conjugated rigid-rod polybenzobisazoles, including three new polymers, were explored by cyclic voltammetry and measurement of the optical dispersion of the refractive index. The electrochemical reduction of the polymers was reversible whereas oxidation was not reversible in accord with the electron deficient nature of the benzobisazole ring. The observed variation of the reduction and oxidation potentials, electron affinity, and ionization potential of the series of polymers was related to the variation in backbone structure. The electron affinity of the polymers was 2.4 to 3.0 eV which indicated that the LUMO energy level was tunable by up to 0.6 eV. The ionization potential (5.2 to 5.7 eV) and associated HOMO level of the polymers was tunable by up to 0.5 eV. The measured wavelength dispersion of the refractive index of the polybenzobisazoles showed that n(lambda = 1064 nm) and n(lambda = 2500 run) were 1.74-2.03 and 1.55-1.95 respectively. The large refractive index variation with molecular structure was satisfactorily accounted for by the competing effects of polarizability and molar volume. These results provide a basis for understanding the electronic, optoelectronic, and optical properties of the conjugated polybenzobisazoles in terms of the underlying molecular and electronic structures. jg

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Document Details

Document Type
Technical Report
Publication Date
Mar 20, 1995
Accession Number
ADA292968

Entities

People

  • John A. Osaheni
  • Samson A. Jenekhe

Organizations

  • University of Rochester

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Absorption Spectra
  • Chemical Synthesis
  • Chemistry
  • Dispersions
  • Electrons
  • Energy Levels
  • Ionization
  • Ionization Potentials
  • Measurement
  • Molecular Structure
  • Optical Materials
  • Optical Properties
  • Polymeric Films
  • Polymers
  • Refractive Index
  • Rigid Rod Polymers
  • Thin Films

Fields of Study

  • Chemistry

Readers

  • Polymer Science and Technology
  • Pulsed Power and Plasma Physics.
  • Spectroscopy.

Technology Areas

  • Microelectronics