Fabrication and Evaluation of Nanoelectrode Ensembles.

Abstract

An electroless deposition procedure for filling the pores in nanoporous filtration membranes with metal (gold) nanowires is described. This method allows us to routinely prepare ensembles of gold nanodisk electrodes in which the nanodisks have diameters as small as 10 nm. Results of electrochemical experiments at ensembles of 30 nm-diameter and 10 nm-diameter gold-disk electrodes are described. The electrochemical response characteristics of these nanoelectrode ensembles are in agreement with predictions of the relevant electrochemical theories. Cyclic voltammetric detection limits for electroactive species at ensembles containing 10 nm-diameter gold disks can be as much as 3 orders of magnitude lower than at a large-diameter gold-disk electrode.

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Document Details

Document Type
Technical Report
Publication Date
Apr 18, 1995
Accession Number
ADA293465

Entities

People

  • Charles R. Martin
  • Vinod P. Menon

Organizations

  • Colorado State University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Absorption Spectra
  • Agreements
  • Chemical Synthesis
  • Chemistry
  • Detection
  • Electrodes
  • Electron Microscopy
  • Electron Transfer
  • Fabrication
  • Materials
  • Measurement
  • Membranes
  • Microscopy
  • Nanomaterials
  • Nanowires
  • Optical Properties
  • Scanning Electron Microscopy

Fields of Study

  • Chemistry

Readers

  • Electrochemical Surface Science
  • Nanoscale Plasmonic Nanotechnology