Syntheses, Characterization, Crystal and Molecular Structures and Solution Properties of Et2Ga(C5H5) and EtGa(C5H5) 2.

Abstract

The compounds Et2Ga(C5H5) and EtGa(C5H5)2 have been prepared by ligand redistribution reactions in pentane solution between appropriate quantities of GaEt3 and Ga(C5H5)3. Both compounds have been fully characterized by elemental analyses, X-ray structural studies, cryoscopic molecular weight studies in benzene solution, mass spectroscopic studies, 1H NMR studies of solutions and 1H NMR studies of the melts. Both compounds exist as pure single compounds in the solid state. jg

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Document Details

Document Type
Technical Report
Publication Date
Jun 19, 1995
Accession Number
ADA295665

Entities

People

  • Charles H. Lake
  • Daniel B. Rosenblum
  • Lynn M. Krajkowski
  • Melvyn Rowen M.R. Churchill
  • O. T. Beachley Jr.

Organizations

  • University at Buffalo

Tags

Communities of Interest

  • Air Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Alkanes
  • Chemical Synthesis
  • Chemistry
  • Crystal Structure
  • Diffraction
  • Diffractometers
  • Equations
  • Exchange Reactions
  • Group 13 Elements
  • Materials
  • Military Research
  • Molecular Weight
  • New York
  • Scattering
  • Spectra
  • United States
  • X Rays

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry