Polymerization of Poly(p-Phenylene Sulfide) from Cyclic Precursor.

Abstract

The objective of this project is to understand the effect of carbon fibers and other high performance reinforcing fibers on the structure of high performance resins such as poly(phenylene sulfide) and epoxies. Of particular interest is the molecular structure/property relationships. Our approach for this project utilized molecular vibrational technique for the understanding of the structure of polymers. Significant scientific conclusions are that we have investigated detailed structural aspects of a cyclic poly(phenylene sulfide) for its crystal structure and polymerization characteristics. As the interest in cyclic compounds as precursors for polymers became strong in recent several years, the conclusion obtained in this study will help evaluate feasibility of using cyclic poly(phenylene sulfide) as potential raw materials for advanced composite materials. We have also studied the state of cure of epoxy resin around an organic fiber using infrared microscopy. With a site specific information on curing, we were able to map the state of cure around a single reinforcing filament, thus enabling the study of the fiber surface on the curing reaction of the matric resin.

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Document Details

Document Type
Technical Report
Publication Date
Oct 18, 1995
Accession Number
ADA300333

Entities

People

  • Hatsuo Ishida
  • Jack L. Koenig

Organizations

  • Case Western Reserve University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Advanced Materials
  • Carbon Fibers
  • Composite Materials
  • Crystal Structure
  • Cyclic Compounds
  • Epoxy Resins
  • Fiber Reinforced Composites
  • Fibers
  • Filaments
  • Materials
  • Mechanical Properties
  • Microscopy
  • Plastics
  • Polymer Matrix Composites
  • Polymers
  • Reinforced Plastics
  • Resins

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Organic Chemistry
  • Polymer Science and Technology
  • Reinforced Composite Materials