Toughening Mechanism in Elastomer-Modified Epoxy Resins. Part 1.

Abstract

Several plaques of Epon 828, cured with piperidine, modified with Hycar(R), CTBN 1300x8, Hycar(R) CTBN 1300X13, and HyCar(R) CTBN 1300X15, and in some cases modified with bisphenol 'A' (BPA), yielded properly toughened epoxies with rubber particle diameters ranging from 0.1 to 10 micrometers. Fracture toughness experiments indicate that toughness was more a function of rubber content than the rubber particle size. Tensile volumetric behavior of the neat resin exhibits two regions: an initial region where the increase in volume strain was due to the Poisson's effect, and a second region where a slower rate of increase in volume strain was due to shear deformation. Tensile volumetric deformation of an elastomer-modified epoxy exhibits the same type of behavior to that of the neat resin at low rates (<3.2 x 10(exp -2/sec). But at very high strain rates, which correspond more closely to the strain rates at the crack tip, there exists an increase in volume strain beyond the Poisson's effect. TEM, SEM and OM studies indicate that the rubber particles had voided. When a thin section from the deformed region is viewed under crossed-polarized light, shear bands are seen connecting voided rubber particles. From this information cavitation and enhanced shear band formation is proposed as the toughening mechanism. jg p131

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1983
Accession Number
ADA305783

Entities

People

  • Albert F. Yee
  • R. A. Pearson

Organizations

  • General Electric

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Electron Microscopy
  • Epoxy Resins
  • Fast Fractures
  • Geometry
  • Low Temperature
  • Materials
  • Materials Processing
  • Measurement
  • Mechanical Properties
  • Mechanical Working
  • Mechanics
  • Microscopes
  • Microscopy
  • Resins
  • Stress Strain Relations
  • Stresses
  • Tensile Stress

Fields of Study

  • Materials science

Readers

  • Plasma Physics.
  • Polymer Science and Engineering.
  • Powder metallurgy of Titanium alloys.