Synthesis and Properties of Vanadium Oxide Aerogel Films.

Abstract

The fine colloid size, high surface area and controllable density of vanadium oxide aerogels make these materials interesting candidates for lithium insertion electrodes. Thin films of vanadium oxide aerogels were prepared using an alkoxide precursor sol and supercritical drying with CO2. Film preparation methods included spin coating of fine aerogel particles suspended in a solvent and dip coating of the precursor sol onto carbon paper substrates. The room temperature electrical conductivity of partially dehydrated materials (V2O5 0.5 H2O) varies from 10(exp -5) S/cm to 10(exp -4) S/cm depending upon the density of the final aerogel. Potential sweep measurements indicate that the films possess good insertion capacity (approx. 2 Li a per V2O5) and can be cycled reversibly. p1

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Document Details

Document Type
Technical Report
Publication Date
Jun 18, 1996
Accession Number
ADA310637

Entities

People

  • Bruce S. Dunn
  • F. Chaput
  • H. P. Wong
  • K. Salloux
  • M. W. Breiter

Organizations

  • University of California, Los Angeles

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Chemistry
  • Coatings
  • Conductivity
  • Dip Coating
  • Electrical Conductivity
  • Electrical Properties
  • Electrodes
  • Films
  • Heat Of Activation
  • Materials
  • Materials Science
  • Measurement
  • Precursors
  • Spin Coatings
  • Substrates
  • Thin Films
  • Vanadium

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Materials Science and Engineering.
  • Thin Film Deposition Science.