Thin-Layer Electrochemical Studies in the Development of a Cycle for the Formation of CdInSe2 by Electrochemical ALE.

Abstract

A thin-layer electrochemical cell (TLEC) was used in the development of a method for the electrodeposition of CuInSe2. Underpotential deposition (UPD) of atomic layers of Cu, In, and Se, as well as layers of Cu2Se, InSe and InSe2 was performed. However, extension of layers of CuInSe2 proved significantly more difficult due to differences in stability of Cu and In. A complexing agent was used to adjust the activity of the Cu, forcing its formal potential to more negative values. The UPD behavior of Cu on an atomic layer of Se, however, appeared to be significantly impeded by the presence of the complexing agent The information obtained in this study is intended to facilitate the development of an Electrochemical ALE cycle for the deposition of CuInS2. Future work will involve studies using an automated flow cell deposition system.

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Document Details

Document Type
Technical Report
Publication Date
Jun 22, 1996
Accession Number
ADA310785

Entities

People

  • John L. Stickney
  • Robert D. Herrick Ii

Organizations

  • University of Georgia

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Cells
  • Chemistry
  • Compound Semiconductors
  • Electrochemical Cells
  • Electrodeposition
  • Electrodes
  • High Temperature
  • Liquid Chromatography
  • Military Research
  • Monomolecular Films
  • New York
  • Schematic Diagrams
  • Semiconductors
  • Solar Cells
  • Solar Energy
  • Ternary Compounds
  • Voltammetry

Fields of Study

  • Materials science

Readers

  • Electrochemical Surface Science
  • Materials Science and Engineering.
  • Thin Film Deposition Science.