Condensed-Phase Processes During Solid Propellant Combustion. V. Further Observations on Depth Profiling of Burned Surfaces of XM39 and M43 Propellants.

Abstract

Samples of XM39 and M43 propellants that have been self-extinguished at low pressures have been examined under a Scanning Electron Microscope (SEM). The results of this examination suggest that the surface layers of burning HMX/RDX propellants consist of a thin, smooth layer presumably made up of binder and its decomposition products. This layer overlies a thicker layer of crystalline, bubble-containing material that is presumably mostly solidified or recrystallized (liquified during combustion) RDX oxidizer. Photoacoustic Fourier Transform Infrared (FTIR) spectra of some burned/extinguished samples of XM39, JA2, and RDX are also reported and discussed. Based on our results to date, presented in this and previous reports, some suggestions for modelers of nitramine propellant combustion are presented. It is suggested that, if practicable, formation and subsequent decomposition of nitrosoamines, such as MRDX and DRDX, should be included in the condensed-phase chemistry models of deflagration of RDX and of RDX-based propellants. Also, the mathematical framework should include provision for formation and growth of bubbles in the liquid layer as a result of both thermal decomposition and vaporization of RDX.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1996
Accession Number
ADA310815

Entities

People

  • J. M. Widder
  • M. A. Schroeder
  • M. S. Miller
  • R. A. Fifer
  • R. A. Pesce-rodriguez

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Burning Rate
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Combustion
  • Composite Propellants
  • Double Base Propellants
  • Liquid Chromatography
  • Materials Laboratories
  • Materials Science
  • Military Research
  • Phase Transformations
  • Propellants
  • Solid Propellants
  • Spectra
  • Transition Temperature
  • Triple Base Propellants

Readers

  • Rocket Propulsion.
  • Thin Film Deposition Science.
  • Underwater engineering and Marine Technology.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene