The Effects of Ferrocenic and Carborane Derivative Burn Rate Catalysts in AP Composite Propellant Combustion: Mechanism of Ferrocene-Catalysed Combustion.

Abstract

The combustion of HTPB/AP propellants containing ferrocene-type and carborane-type burn rate catalysts was examined. The ferrocenic catalysts are good burn rate enhancers, but the carborane-type compounds showed little improvement, even at 3% catalyst concentration. An order of relative catalyst effectiveness was established for 1% catalyst concentration at 20 deg C. Examination reveals the enhancing effect of 1% Catocene is approximately equivalent to 0.5% Butacene. Characteristic surface features observed for the carborane- catalysed propellants contrast to those for the ferrocene-catalysed propellants. For ferrocene-catalysed combustion, the experimental evidence is in favour of a mechanism whereby the ferrocenic catalyst acts in the binder to catalyse the heterogeneous reactions between the binder and the AP at the binder/oxidiser interface. The evidence includes the following: (1) Enhanced burn rates of the Butacene propellant over the Catocene propellant, both propellants containing the same amount of iron in the ferrocenic catalysts; (2) Fe particles dispersed in the binder of the quenched propellant surface; (3) undercuttings along the boundaries of surface AP particles; and (4) the convex, protruding (sometimes apparently intact) AP particle surface. There was no evidence of the catalyst promoting surface AP decomposition reactions. p50

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1995
Accession Number
ADA311583

Entities

People

  • Thanh Nguyen

Organizations

  • Defence Science and Technology Group

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Additives (Chemicals)
  • Aluminized Propellants
  • Aluminum
  • Aluminum Oxides
  • Chemical Synthesis
  • Chemistry
  • Combustion
  • Composite Materials
  • Composite Propellants
  • Electron Microscopy
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Measurement
  • Oxides
  • Propellants

Readers

  • Chemistry (specifically Chemical Fluorescence)
  • Combustion and Flow Dynamics.
  • Organic Chemistry