Transition Metal Complex Superconductors by Electrocrystallization. Nonmetallic and Bimetallic Chalcogen-Rich, Extensively Conjugated and Planar Complexes for Highly Electrically Conducting Materials.

Abstract

A series of monometallic and bimetallic transition metal complexes have been synthesized for incorporation into highly conductive and potentially superconductive materials. Studies of Ni(dmit)2(C(+))(x), as a function of cation (C(+)) type, have allowed elucidation of the effect of structure on electronic properties. A new class of bimetallic tetrathiooxalate (tto) bridged compounds were discovered that form new synthetic conductors. For example, the reaction of (Bu4N)2?ttoNi(dmit)2! with (TTF)3(BF4)2 led to a material with a conductivity of 0.4 S/cm. A full study of seven new bimetallic, and one new tetrametallic, complex has been carried out with single crystal X-ray structures determined.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Sep 23, 1996
Accession Number
ADA317220

Entities

People

  • John R. Reynolds

Organizations

  • University of Florida

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Advanced Materials
  • Charge Transfer
  • Chemistry
  • Conductivity
  • Coordination Complexes
  • Diffraction
  • Energy Bands
  • Inorganic Chemistry
  • Materials
  • Materials Engineering
  • Materials Science
  • Metals
  • Optical Properties
  • Transition Metals
  • Voltammetry
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Chemistry

Readers

  • Nanofabrication and Microfabrication.
  • Organic Chemistry
  • Superconducting Magnet Technology

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene