A Facility for the Attribute-Based Vapor Phase Processing of Multilayers and Coatings

Abstract

An electron beam deposition system suitable for the intelligent processing of oxide films and coatings has been designed and constructed. The three major features include (1) a heated substrate with a rotating stage (2) magnetically rastered e-beam dual sources, (3) four sub-systems for measuring film properties either in situ or post situ. The latter include: (a) an infrared imaging system, (b) a beam curvature apparatus for stress measurement, (c) an atomic force microscope to quantify topography. The system is being applied to oxide films relevant to thermal barrier applications (notably ZrO2) as well as alumina, ytrria and other oxides suitable for oxidation protection. The deposited films are being subject to a measurement protocol that determines their residual strain state, their fracture toughness and their adhesion to alloy substrates.

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Document Details

Document Type
Technical Report
Publication Date
Jun 26, 1997
Accession Number
ADA330747

Entities

People

  • Anthony G. Evans

Organizations

  • Harvard College

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies
  • Sensors

DTIC Thesaurus Topics

  • Adhesion
  • Coatings
  • Curvature
  • Detectors
  • Electron Beams
  • Energy
  • Energy Management
  • Films
  • Geometry
  • Materials
  • Measurement
  • Microscopes
  • Oxide Films
  • Oxides
  • Physical Vapor Deposition
  • Substrates
  • Vapor Phases

Fields of Study

  • Physics

Readers

  • Materials Science and Engineering.
  • Nanoscale Plasmonic Nanotechnology
  • Pulsed Power and Plasma Physics.

Technology Areas

  • Directed Energy
  • Directed Energy - Pulsed-Laser Deposition
  • Microelectronics
  • Microelectronics - Graphene