Effect of Precrack "Halos" on KIc Determined by the Surface Crack in Flexure Method

Abstract

The surface crack in flexure (SCF) method, which is used to determine the fracture toughness of dense ceramics necessitates the measurement of precrack sizes by fractographic examination. Stable crack extension may occur from flaws under ambient room-temperature conditions, even in the relatively short time under load during fast fracture strength or fracture toughness testing. In this paper, fractographic techniques are used to characterize evidence of stable crack extension, a halo, around Knoop indentation surface cracks. Optical examination of the fracture surfaces of a high-purity Al2O3, an AlN, a glass-ceramic, and a MgF2 revealed the presence of a "halo" around the periphery of each precrack. The halo in the AlN was merely an optical effect due to crack reorientation, while the halo in the MgF2 was due to indentation-induced residual stresses initiating crack growth. However, for the Al2O3 and the glass-ceramic, environmentally assisted slow crack growth (SCG) was the cause of the halo. In the latter two materials, this stable crack extension must be included as part of the critical crack size in order to determine the appropriate fracture toughness.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1997
Accession Number
ADA335068

Entities

People

  • George D. Quinn
  • Jeffrey J. Swab

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics
  • Air Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Boundaries
  • Cantilever Beams
  • Ceramic Materials
  • Failure Mode And Effect Analysis
  • Fast Fractures
  • First Principles Calculations
  • Fracture (Mechanics)
  • Materials
  • Materials Science
  • Materials Testing
  • Measurement
  • Mechanics
  • Residual Stress
  • Stresses
  • Structural Ceramics
  • Technical Ceramics
  • Test Methods

Readers

  • Astronomy/Astrophysics
  • Powder metallurgy of Titanium alloys.
  • Structural Health Monitoring of Composite Structures.