Oxygen Ion Conductors Prepared with Nanosize Particles

Abstract

The instrumentation acquired from this grant consists of two atomic force microscopes (from Park Scientific and Molecular Imaging) and a particle size analyzer (from Micromeritics). The atomic force microscopes are complementary in terms of their operation and use the same controller and software. The Park Scientific instrument has been used to characterize the microstructure development of thin films of the oxygen ion conductor, BICUVOX (Bi(2)V(0.9)Cu(0.1)O(5.35)) over the temperature range from 550 to 800 deg C. Grain growth occurring in the film appears to he two-dimensional in nature. The Molecular Imaging AFM is designed for characterizing the topology of liquid/solid interfaces. This instrument has been used to image the surface of a lithium battery cathode material, V2O5, during lithium intercalation. The particle size analyzer has been used to characterize the particle size and particle size distribution of powders of various materials produced by the Pechini method as a function of heat treatment temperature.

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Document Details

Document Type
Technical Report
Publication Date
Mar 23, 1998
Accession Number
ADA341794

Entities

People

  • Bruce Dunn
  • J. D. Mackenzie

Organizations

  • University of California, Los Angeles

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Analyzers
  • Chemical Synthesis
  • Chemistry
  • Electrochemical Cells
  • Electron Microscopy
  • Films
  • Grain Growth
  • Grain Size
  • Lithium Batteries
  • Materials
  • Materials Science
  • Microscopes
  • Particle Size
  • Particles
  • Thin Films
  • Transition Metals
  • Two Dimensional

Fields of Study

  • Materials science
  • Physics

Readers

  • Aerosol Science/Aerosol Physics
  • Electrochemical Engineering/ Fuel Cell Technologies
  • Thin Film Deposition Science.