High-Temperature Heterogeneous Redox Catalysis for NOx Abatement

Abstract

This Phase I SBIR program was directed towards the synthesis, characterization, and determination of preferred catalyst compositions for the high-temperature direct (reagentless) decomposition of nitrogen oxides in exhaust streams. Phase I results showed clearly that significant persistent (nontransient) activity (35% removal) for direct deNO(x) (at > 500 deg C) could be attained in helium at space velocities of ^1,000,000 per h (3.6ms residence time) over a brownmillerite catalyst supported on a powdered ceramic (yttria-stabilized zirconia) representative of thermal barrier coatings, in the presence of 16% O2, absent of any reagent. This catalyst, when unsupported, showed persistent activity (27% removal at 500,000 per h for at least 6 hours and at least 140 hours at 50,000 per h). Significant activity was measured at up to 1,000 deg C. These catalysts also possessed exceptional activity for the combustion of propane and propylene as well as measurable activity for oxidation of CO. Preliminary results showed tolerance to feedstream CO2 (10%) and SO2 (10ppm). Results point clearly to probable attainment of Air Force's Phase II targets of 50% removal in millisecond residence time regimes and retention of 50% of initial activity after 500 hours.

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Document Details

Document Type
Technical Report
Publication Date
Jan 23, 1998
Accession Number
ADA344818

Entities

People

  • A. F. Sammells
  • J. Heidrick
  • J. Mitchel
  • J. White
  • S. Roark

Tags

Communities of Interest

  • Energy and Power Technologies
  • Sensors

DTIC Thesaurus Topics

  • Chemistry
  • Combustion
  • Detectors
  • Dielectric Gases
  • Gas Turbines
  • High Temperature
  • Hydroxides
  • Jet Engines
  • Mass Spectrometers
  • Mass Spectrometry
  • Measurement
  • Nitrogen Oxides
  • Oxidation
  • Spectra
  • Spectrometry
  • Spectroscopy
  • Transition Metals

Readers

  • Internal Combustion Engine (ICE) Technology.
  • Mathematics or Statistics
  • Powder metallurgy of Titanium alloys.

Technology Areas

  • Space
  • Space - Hall-Effect Thruster