Macrocyclic Radiochelates for Antibody Imaging and Therapy of Breast Cancer.

Abstract

Conjugation of bifunctional chelating agents allows monoclonal antibodies (mAbs) to be labeled with radiometals for delivery of diagnostic or therapeutic radiation to primary breast tumors or metastatic disease. Physiologically stable radiometal chelates, such as those of 1,4,7,10- tetraazacyclododecane N,N',N",N"'-tetraacetic acid (DOTA), are desirable to reduce dose-limiting radiation toxicity to normal tissues. Two new classes of DOTA derivatives, maleimidocysteineamido-DOTA derivatives and hydrazido-DOTA derivatives, were synthesized and conjugated, respectively, to reduced interchain disulfide bonds and oxidized carbohydrate residues of the anti-carcinoembryonic antigen mAbs cT84.66 and ZCE025. Conjugates of cT84.66 prepared with maleimide derivatives of DOTA exhibited near-quantitative labeling with the imaging radiometal. In and the therapy radiometal 90Y, quantitative immunoreactivity, and linker-specific cleavage reactions which were considerably faster at pH 7.4 than at pH 5.4. Biodistribution studies demonstrated that this property imparted favorable tumor uptake and normal tissue clearance to radiolabeled cT84.66. Conjugation of oxidized cT84.66 with hydrazido-DOTA resulted in extensive antibody aggregation and low radiometal labeling yields. Conjugation of oxidized ZCE025 with hydrazido-DOTA, carbohydrazido-DOTA, and hydrazidocysteineamido-DOTA was also unsuccessful. It is possible that modification of the ZCE025 conjugation procedure or use of a CT84.66 construct with a genetically engineered oligosaccharide will allow successful attachment and radiometal labeling of the hydrazido-DOTA derivatives.

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1998
Accession Number
ADA349597

Entities

People

  • Michael R. Lewis

Tags

DTIC Thesaurus Topics

  • Amines
  • Amino Acids
  • Breast Cancer
  • Chemical Synthesis
  • Chemistry
  • Colon Cancer
  • Mass Spectrometry
  • Medical Personnel
  • Organic Chemistry

Fields of Study

  • Chemistry

Readers

  • Data Mining and Knowledge Discovery.
  • Molecular and Cellular Biochemistry
  • Organic Chemistry

Technology Areas

  • Biotechnology
  • Biotechnology - Cancer Biotech