Evaluation of Hydroxyethane Diphosphonic Acid (HEDPA) as Metal Cleaning Agent Using Chemical and Electrochemical Test Methods: Part 2

Abstract

In order to evaluate the adaptability of hydroxyethane diphosphonic acid (HEDPA) as an environmentally benign alternative rust removal agent, a systematic investigation is being carried out. The effectiveness of HEDPA was thoroughly investigated as a function of acid concentration in the range 2 - 100 vol% and at different temperatures in the temperature range 27 - 60 deg C. The results suggest that the acid HEDPA is very effective in the rust removal process. The rate of rust removal by HEDPA is strongly dependent on the acid concentration and the solution temperature. Once an optimum threshold is reached further increase in either the acid concentration and/or temperature has a negative effect on the reaction kinetics. Chemical treatment of rusted steel samples with concentrated HEDPA solution (concentration range 5 - 100 vol.% HEDPA) has produced rust free steel samples with very rough surface topography. Prolonged treatment of samples with HEDPA allows the re-deposition of the reaction products onto the cleaned sample surface. The reaction product contains a mixture of various higher order iron phosphates.

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 1998
Accession Number
ADA353718

Entities

People

  • A. S. Rao
  • J. N. Murray

Organizations

  • Naval Surface Warfare Center Carderock Division

Tags

Communities of Interest

  • Advanced Electronics
  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Adhesion
  • Base Metal
  • Body Weight
  • Chemical Analysis
  • Chemical Kinetics
  • Chemical Reactions
  • Chemistry
  • Crystal Structure
  • Diffraction
  • Heat Of Activation
  • Kinetics
  • Materials
  • Precipitation
  • Test And Evaluation
  • Test Methods
  • X Rays
  • X-Ray Diffraction

Readers

  • Materials Science and Engineering.
  • Positioning, Navigation, and Timing (PNT) Technology.
  • Surface Coatings Technology.