Assessment of Exposure to Sensitizing Rosin-derived Compounds from Electronics Soldering

Abstract

Exposure potential for rosin-derived compounds, including volatile and semivolatile organic compounds produced during electronics soldering operations using rosin-based fluxes and rosin core solders, was investigated. A reaction system was constructed for trapping emission products. Particulate matter was collected on filters, and volatile organic compounds were collected on sorbent tube media for analysis by gas chromatography/mass spectrometry (GC/MS). Comparisons were made between reaction system samples and actual breathing zone samples collected during soldering operations. Other work included: (1) A protein conjugation/haptenation mechanism for 7-oxodehydroabietic acid, an oxidized resin acid compound present in aerosol produced by heating rosin flux, (2) Identification of low molecular weight aldehydes in soldering emissions using gas chromatography/mass spectrometery (GC/MS), (3) In vitro studies of resin acid metabolism to identify mammalian metabolites produced from dehydroabietic acid, and (4) A rapid method for analyzing headspace sampling of aldehydes using solvating gas chromatography (SGC). This project provided information regarding the specific compounds generated during rosin heating in electronic soldering applications. A possible biological mechanism was shown for sensitization to a resin acid present in aerosol produced during heating rosin flux. The work described may prove useful in producing an exposure standard for contaminant sampling during electronics soldering operations.

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Document Details

Document Type
Technical Report
Publication Date
Nov 06, 1998
Accession Number
ADA355713

Entities

People

  • Christopher R. Bowerbank
  • Milton L. Lee

Organizations

  • Brigham Young University

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical

DTIC Thesaurus Topics

  • Aldehydes
  • Carboxylic Acids
  • Chemical Compounds
  • Chemical Synthesis
  • Chemistry
  • Chromatography
  • Gas Chromatography
  • Liquid Chromatography
  • Mass Spectrometry
  • Optical Materials
  • Organic Chemistry
  • Organic Compounds
  • Rodents
  • Skin Diseases
  • Spectrometry

Fields of Study

  • Environmental science

Readers

  • Agricultural Chemistry/Soil Science
  • Electrical Engineering
  • Surface Coatings Technology.

Technology Areas

  • Microelectronics