Self-Assembled Aggregates of Rod-Coil Block Copolymers and Their Solubilization and Encapsulation of Fullerenes

Abstract

Amphiphilic Poly(phenylquinoline)- block-polystyrene rod-coil diblock copolymers have been observed to self-organize into robust, micrometer-scale, spherical, vesicular, cylindrical, and lamellar aggregates from solution. These diverse aggregate morphologies were observed at each composition but their size scale decreased with decreasing fraction of the rigid-rod block. Compared to coil-coil block copolymer micelles, the present aggregates are larger by about two orders of magnitude and have aggregation numbers of over 10 to the 8th power. The spherical and cylindrical aggregates have large hollow cavities. Only spherical aggregates with aggregation numbers in excess of 10 to the 9th power were formed in the presence of fullerenes (C60, C70) in solution, resulting in the 10 solubilization and encapsulation of over 10 to the 10th power fullerene molecules per aggregate.

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Document Details

Document Type
Technical Report
Publication Date
Nov 16, 1998
Accession Number
ADA356432

Entities

People

  • Samson A. Jenekhe
  • X. L. Chen

Organizations

  • University of Rochester

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Assembly
  • Biomedical And Dental Materials
  • Block Copolymers
  • Chemical Engineering
  • Chemistry
  • Copolymers
  • Electron Microscopy
  • Encapsulation
  • Fullerenes
  • Materials
  • Materials Science
  • Microcapsules
  • Molecules
  • Polymers
  • Self Assembly
  • Spectra
  • Three Dimensional

Readers

  • Mathematics or Statistics
  • Nanocomposite Materials Science

Technology Areas

  • Microelectronics