Complex Impedance Studies Of Proton-Conducting Membranes

Abstract

Complex impedance studies have been carried out on Dow 800, Dow 1000 and Nafion 117 membranes at various water contents and a variety of temperatures and pressures. At room temperature and pressure a gradual decrease in electrical conductivity with decreasing water content is observed. Apparent activation volumes as large as 54 cm3/mol are obtained. In addition, there is a tendency for smaller equivalent weights (same side chains) or larger side chains to have larger activation volumes. Additionally, ambient-pressure, variable-temperature 2H T1 and linewidth measurements imply a heterogeneous environment of the water molecules. Proton pulsed field gradient NMR studies in saturated Dow membranes verify the expectation that ionic conductivity is determined primarily by diffusion of water molecules.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1999
Accession Number
ADA365266

Entities

People

  • C. A. Edmondson
  • John J. Fontanella
  • M. C. Wintersgill
  • M. E. Chapman
  • P. E. Stallworth

Organizations

  • United States Naval Academy

Tags

DTIC Thesaurus Topics

  • Conductivity
  • Diffusion
  • Electrical Conductivity
  • Environment
  • Films
  • Fluorinated Hydrocarbons
  • Fluoropolymers
  • Frequency
  • High Pressure
  • Impedance
  • Materials
  • Measurement
  • Molecules
  • New York
  • Pressure Measurement
  • United States
  • United States Naval Academy

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Materials Science and Engineering.