Titanium Carbosulfides and the Fracture Toughness of Ultra High Strength Steels

Abstract

The objectives of this work were to calculate from first principles the work of adhesion associated with the steel-MnS and steel-Ti2CS interfaces and to examine with transmission electron microscopy void nucleation at particles of MnS and particles of Ti2CS in steel. The motivation for this work was the observation that gettering sulfur as Ti2CS rather than as MnS leads to doubling and even tripling of the fracture toughness of some ultra-high strength steels and that these improvements in toughness were believed to be due to particles of Ti2CS being much more resistant to void nucleation than particles of MnS. The results are as follows. Using the LKKR approach the bulk properties and surface energies of MnS and F.C.C. iron were calculated as was the interface energy of a MnS-steel interface. With these the results the work of adhesion for this interface was determined. The bulk properties of Ti2CS were determined but we were unable to obtain reasonable results for a Ti2CS-steel interface. The investigations of void nucleation at particles of MnS and Ti2CS in two different heats of an austenitic 0.07/30Ni steel were surprising. In this material it was found that voids were first nucleated at both inclusion types at strains as low as 0.20. It had been expected that voids would be first nucleated at the particles of MnS at these low strains but that voids would not be observed at the particles of Ti2CS until the strains had exceeded at least one.

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Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1999
Accession Number
ADA371454

Entities

People

  • Warren M. Garrison Jr.

Organizations

  • Carnegie Mellon University

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Compounds
  • Chemistry
  • Crystal Structure
  • Electron Microscopy
  • Fermi Levels
  • Ferrium
  • Materials
  • Materials Science
  • Mechanical Properties
  • Mechanical Working
  • Mechanics
  • Microscopes
  • Microscopy
  • Solid State Physics
  • Tensile Properties
  • Tensile Strength
  • Three Dimensional

Fields of Study

  • Materials science

Readers

  • Aerosol Science/Aerosol Physics
  • Materials Science (Mechanical Engineering).
  • Powder metallurgy of Titanium alloys.

Technology Areas

  • Microelectronics