Degree of Cure, Heat of Reaction, and Viscosity of 8552 and 977-3 HM Epoxy Resin

Abstract

The heat of reaction, degree of cure, and viscosity of Hexcel 8552 and Cytec Fiberite 977-3 HM neat resins were measured using a modulated differential scanning calorimeter and a rheometric digital analyzer. Expressions were developed using isothermal tests for correlating the rate of degree of cure and the viscosity with the degree of cure using a Lee, Loos, and Springer approach. The models were exercised to predict the kinetic behavior of the resins using respective manufacturer cure cycles. Data were collected and good correlation was found with the model. In addition, kinetic behaviors of these systems were compared to Hercules 3501-6 data. A second study was also performed to investigate cure models developed based on neat and prepreg forms of the resin. Vastly different viscosity behaviors were found indicating further physical insights are necessary to account for fiber/resin content and material properties difference.

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Document Details

Document Type
Technical Report
Publication Date
Mar 10, 2000
Accession Number
ADA377439

Entities

People

  • A. Vizzini
  • F. Arnold
  • R. Boswell
  • S. J. Claus
  • S. J. Ng

Organizations

  • Naval Air Warfare Center

Tags

Communities of Interest

  • Air Platforms
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Aerial Warfare
  • Aircrafts
  • Composite Materials
  • Epoxy Resins
  • Equations
  • Heat Energy
  • Heat Of Activation
  • Heat Of Reaction
  • Laminates
  • Materials
  • Measurement
  • Plastics
  • Reinforced Plastics
  • Resins
  • Scanning
  • Thermosetting Plastics
  • Viscosity

Fields of Study

  • Materials science

Readers

  • Computational Modeling and Simulation
  • Polymer Science and Engineering.
  • Reinforced Composite Materials