Examination of Oxide Scales on Heat Resisting Alloys

Abstract

Twelve iron, nickel, and cobalt heat resisting alloys were cyclic furnace oxidation tested at from 1400 degrees to 2200 degrees F (1033 to 1478 K) for from 4 to 600 hours. Retained oxide scales and spall were identified using X-ray diffraction combined with X-ray fluorescence analysis. Metallography clarified scale growth sequences. After 600 hours at 2000 degrees F (1366 K), the condition most studied, the best oxidation resistance, as reflected by weight change and spall weight, was exhibited by alloys forming single oxide scales of Al2O3 or Cr2O3. For alloys that developed multioxide scales, spinel constituent composition or lattice parameter did not correlate with oxidation resistance.

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Document Details

Document Type
Technical Report
Publication Date
Feb 01, 1969
Accession Number
ADA379999

Entities

People

  • Carl E. Lowell
  • Salvatore J. Grisaffe

Organizations

  • National Aeronautics and Space Administration

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Alloys
  • Aluminum Oxides
  • Body Weight
  • Chemical Analysis
  • Chemical Synthesis
  • Chemistry
  • Chromium
  • Crystal Lattices
  • Crystal Structure
  • Diffraction
  • Heat Resistant Alloys
  • High Temperature
  • Materials
  • Oxidation
  • Oxidation Resistance
  • Solid Solutions
  • X Rays

Fields of Study

  • Materials science

Readers

  • Combustion science or combustion engineering.
  • Powder metallurgy of Titanium alloys.