The Mechanism and Dynamics of Explosive Combustion in Aerosol Fuels

Abstract

This project investigates the explosive combustion of aerosol fuels using a single particle mass spectrometer. Initiating explosive reactions of small samples (-l0(-12) grams) in vacuum allows the intermediate products of the reaction to escape into a collisionless region where we detect them using laser spectroscopy. Recent results from our laboratory explore the mechanism of amine sensitization in nitromethane. We initiate the decomposition of nitromethane/diethylamine aerosols using a CO(2) laser and observe the intermediates of the reaction using laser ionization coupled with time-of-flight mass spectroscopy. The laser ionization source is a vacuum-ultraviolet laser developed using funds from this grant, and it enables near threshold ionization of most radical reaction intermediates. We find that reactions of the aci-anion of nitromethane, formed in an acid-base equilibrium with the amine, are critical in the sensirization mechanism.

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Document Details

Document Type
Technical Report
Publication Date
Aug 15, 2000
Accession Number
ADA381447

Entities

People

  • Roger E. Miller
  • Tomas Baer

Organizations

  • University of North Carolina at Chapel Hill

Tags

Communities of Interest

  • Counter IED
  • Human Systems

DTIC Thesaurus Topics

  • Acid-Base Equilibrium
  • Chemical Reaction Properties
  • Chemical Reactions
  • Combustion
  • Decomposition
  • Explosives
  • Frequency Combs
  • Ionization
  • Laser Applications
  • Laser Beams
  • Lasers
  • Mass Spectrometers
  • Mass Spectrometry
  • Spectrometers
  • Spectrometry
  • Spectroscopy
  • Ultraviolet Lasers

Fields of Study

  • Physics

Readers

  • Molecular Photonics/Laser Physics
  • Organic Chemistry
  • Rocket Propulsion.

Technology Areas

  • Directed Energy