The Polymer Chemistry of Butatrienes and Their Potential as Precursors of Novel Polyacetylenes

Abstract

In this work, we explore novel approaches to new polymers the poly(butyne-l,4-diyl). These are synthsized from 1,2,3-butatrienes, highly unsaturated monomers. Tetrasubstituted systems bearing bulky aliphatic substitutents can be polymerized under controlled conditions. The tetramethyl system cannot be controlled. Using diphenyl substitutents, we have developed a new approach to the synthesis of soluble polyacetyelenes. Using 1,4-diphenylsubstituted butatrienes, we polymerize these monomers to form a non-conjugated poly(l,4-diphenyl-2- butyne-l,4-diyl) . This soluble, processable materials can be converted to the conjugated (poly(diphenylacetyelen-ait-acetylene) for through the application of strong protic bases. we provide synthesic procedures and characterization of both the precursor and final polymers.

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Document Details

Document Type
Technical Report
Publication Date
Feb 06, 2001
Accession Number
ADA386720

Entities

Organizations

  • Howard University

Tags

Communities of Interest

  • Advanced Electronics
  • C4I

DTIC Thesaurus Topics

  • Acetylenes
  • Alkanes
  • Alkynes
  • Chemical Synthesis
  • Chemistry
  • Films
  • Macromolecules
  • Magnesium Compounds
  • Materials
  • Organic Chemistry
  • Polymer Chemistry
  • Polymers
  • Thin Films

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry
  • Polymer Science and Technology