Design and Synthesis of Inorganic/Organic Hybrid Microstructures

Abstract

Vanadium oxide/polypyrrole (V2O5/PPy) hybrid aerogels were prepared using three different strategies. These approaches were focused on either sequential or consecutive polymerization of the inorganic and organic networks. The hybrid microstructure differed greatly depending on which synthesis approach was used. When the inorganic and organic precursors were allowed to polymerize simultaneously, the resulting gels exhibited a nanometer scaled microstructure with a homogeneous distribution of the PPy and the V2O5. Through this route, a suitable microstructure and composition for a lithium secondary battery cathode were obtained. For the full benefit of the PPy phase to be achieved, a suitable doping procedure is still required to oxidize the PPy into its high conductivity state while preserving the inorganic structure.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Jun 25, 2001
Accession Number
ADA391626

Entities

People

  • Bruce Dunn
  • John H. Harreld
  • Linda F. Nazar

Organizations

  • University of California, Los Angeles

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Alcohols
  • Chemical Compounds
  • Chemical Synthesis
  • Chemistry
  • Composite Materials
  • Conductive Polymers
  • Conductivity
  • Ethylene Glycol
  • Materials
  • Materials Science
  • Measurement
  • Microstructure
  • Nanocomposites
  • Organic Chemistry
  • Physical Properties
  • Polymers
  • Transition Metals

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Nanocomposite Materials Science
  • Organic Chemistry