Transport of Ions and Electrostatic Interactions in Thermoresponsive Poly (N-Isopropylacrylamide-co-Acrylic Acid) Hydrogels: Electroanalytical Studies

Abstract

To study transport phenomena and electrostatic interactions in negatively charged poly(N-isopropylacrylacrylamide-co-acrylic acid) hydrogels, NIPA-AA, electroanalytical experiments with two positively charged probes, ferrocenylmethyltrimethylammonium, FcTMA(+), and hexaammineruthenium(III), Ru(NH3)6(3+), cations were performed, and the results compared with those for an uncharged electroactive probe, 1,1'-ferrocenedimethanol, Fc(MeOH)2. Steady-state voltammetry and chronoamperometry at platinum disk microelectrodes were used to determine diffusion coefficients of those probes. For temperatures below the volume phase transition of a gel, there are not significant differences in the transport behavior of cationic and uncharged probes. After the volume phase transition occurs and the gel collapses, the diffusion coefficients of all probes decrease, the change in diffusion coefficient is more pronounced for cationic probes than for a neutral probe, and depends on the charge of the cationic probe. Changes in concentration of cationic species in collapsed NIPA-AA gels were detected as a result of the volume phase transition.

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Document Details

Document Type
Technical Report
Publication Date
Jul 15, 2001
Accession Number
ADA392494

Entities

People

  • Chaoran Ma
  • M. Ciszkowska
  • Wei Zhang

Organizations

  • Brooklyn College

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Acids
  • Acrylic Acid
  • Aqueous Solutions
  • Chemistry
  • Coefficients
  • Diffusion
  • Diffusion Coefficient
  • Equations
  • Gels
  • Heat Of Activation
  • Materials
  • Measurement
  • Phase Transformations
  • Steady State
  • Transition Temperature
  • Transitions
  • Voltammetry

Fields of Study

  • Chemistry

Readers

  • Electrochemical Surface Science
  • Plasma Physics.