High Resolution XPS Analysis of New Lubricants and Materials for Tribology Under Extreme Conditions

Abstract

A high resolution x-ray photoemission spectrometer has been purchased for study of the chemistry of vapor phase lubricants and new tribological materials such as quasicrystals. Typical vapor phase lubricants are compounds such as tricresylphosphate which react with iron surfaces to form lubricating films at high temperatures. Understanding the mechanism by which they decompose on surfaces to form these films is central to developing new VP lubricants or improving the performance of existing VP lubricants. Because of their complexity, high resolution spectroscopy is needed to follow the course of their reactions on surfaces. Quasicrystals are also materials which have potential for use as low friction coatings at high temperatures. These are complex alloys with three or more components which, because of their complexity would benefit from study using high resolution XPS. Understanding the kinetics of their oxidation is important to understanding their performance as high temperature oxidation resistant low friction coatings. The XPS equipment needed for these studies has been purchased and a new ultra-high vacuum chamber is being constructed to house the components of this spectrometer.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 2001
Accession Number
ADA392758

Entities

People

  • Andrew J. Gellman

Organizations

  • Carnegie Mellon University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Chambers
  • Chemical Engineering
  • Chemistry
  • Engineering
  • Films
  • Friction
  • High Resolution
  • High Temperature
  • High Vacuum
  • Instrumentation
  • Lubricants
  • Lubricating Films
  • Materials
  • Spectrometers
  • Spectroscopy
  • Tribology
  • Vapor Phases

Readers

  • Semiconductor Device Technology
  • Tribology (the study of the boundary interaction between sliding surfaces, lubrication, wear and friction).