High-Rate Sputter-Deposited Tantalum Coatings on a Steel Liner for Wear and Erosion Mitigation

Abstract

A prototype, rifled steel liner of 20-min inside diameter was coated with -50 to 125 micronmeter tantalum at -22.6 micronmeter/hour in krypton gas using a triode-sputter system. It was test fired with l5OO rounds for the mitigation of high-temperature and pressure wear and erosion. Growth surface analysis showed predominately alpha-phase and minimal beta-phase surface tantalum. Area detector images showed near random, slight preferred (211) crystalline orientation. X-ray diffraction revealed a thin layer of surface zinc oxide and copper firing debris on the coating surface. Compressive surface residual stress peaked near the center of the tube. Photomicrograph metallurgical examination showed general good adhesion in major parts of the bulk coatings, along with a thin layer of beta-phase nucleation, and alpha-phase or mixed alpha- and beta-phase grain growth. There was excellent behavior in soft and ductile a-tantalum areas, but cracking and disbonding occurred in beta-tantalum areas. Coating liftoff and coating loss occurred most frequently in land/groove transition and land areas, less in groove areas. Near the breech end where no coating was sputtered, the steel substrate suffered extensive cracking and environmentally-assisted heat damages.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 2001
Accession Number
ADA393621

Entities

People

  • D. W. Matson
  • D. Windover
  • Jason Cox
  • M. Audino
  • S. L. Lee

Organizations

  • United States Army Armament Research, Development and Engineering Center

Tags

Communities of Interest

  • Advanced Electronics
  • Weapons Technologies

DTIC Thesaurus Topics

  • Adhesion
  • Body Weight
  • Coatings
  • Detectors
  • Diffraction
  • Grain Growth
  • High Temperature
  • Mechanical Properties
  • Modulus Of Elasticity
  • Orientation (Direction)
  • Physical Properties
  • Refractory Metals
  • Residual Stress
  • Stresses
  • Transitions
  • X Rays
  • X-Ray Diffraction

Readers

  • Materials Science (Mechanical Engineering).
  • Surface Engineering/Surface Coating Technology.
  • Thin Film Deposition Science.