Rapid Vapor Deposition of Millimeters Thick Optically Transparent Solid Parahydrogen Samples for Matrix Isolation Spectroscopy

Abstract

We report a new method for rapid in-vaccuum deposition of millimeters thick solid parahydrogen (pH2) samples which are remarkable for their excellent optical qualities. Infrared and Raman spectra indicate a very low orthohydrogen content, and a mixed hcp/fcc polycrystalline structure for as-deposited samples. Annealing to 4.5 K converts the samples to polycrystalline hcp. Our approach allows for the efficient trapping and isolation of atomic and molecular dopants by conventional matrix isolation techniques. The increased optical path lengths offer pronounced improvements in the quality of spectroscopic data. We have also observed a variety of novel induced IR absorptions of the pH2 matrix host itself; transitions induced by the presence of trapped atoms, molecules, and ions.

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Document Details

Document Type
Technical Report
Publication Date
Nov 03, 1997
Accession Number
ADA398027

Entities

People

  • Mario E. Fajardo
  • Simon Tam

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Ablation
  • Absorption
  • Absorption Spectra
  • Air Force
  • Air Force Research Laboratories
  • Crystal Structure
  • Films
  • Flow Rate
  • High Resolution
  • Lasers
  • Materials
  • Raman Scattering
  • Raman Spectra
  • Scattering
  • Spectra
  • Spectroscopy
  • Vapor Deposition

Readers

  • Molecular Photonics/Laser Physics
  • Semiconductor Device Technology
  • Thin Film Deposition Science.