Power and Efficiency Advancements for Low Rate - Long Endurance Semi-Fuel-Cells

Abstract

The characterization and use of a palladium and iridium catalyst combination on several cathode substrates (carbon paper, porous nickel, titanium dioxide, carbon fibers) are described The Pd/Ir combination outperforms palladium alone or iridium alone on all of the substrates as determined by catalyst deposit stability, polarization curve Tafel slope and onset potential. Scanning electron microscopy (SEM), energy dispersive spectrometry (EDS), and transmission electron microscopy (mM) were used to establish the composition and structure of palladium and iridium clusters on the cathode substrate surfaces. Cyclic voltammetry was employed as the method of choice for deposition; however, constant potential deposition was also investigated. Several deposition parameters were investigated including deposition range, scan rate, and number of cycles. This report describes the optimum deposition conditions and the best catalyzed substrate as tested in a metal-hydrogen peroxide semi-fuel cell.

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Document Details

Document Type
Technical Report
Publication Date
Sep 30, 2002
Accession Number
ADA406734

Entities

People

  • Russell R. Bessette

Organizations

  • University of Massachusetts

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Carbon Fibers
  • Catalysts
  • Cells
  • Chemistry
  • Current Density
  • Data Acquisition
  • Electrochemical Cells
  • Electrodes
  • Electron Microscopes
  • Electron Microscopy
  • Energy
  • Fuel Cells
  • Hydrogen
  • Materials
  • Microscopes
  • Microscopy
  • Scanning Electron Microscopy

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Thin Film Deposition Science.

Technology Areas

  • Biotechnology
  • Microelectronics
  • Microelectronics - Graphene