Characterization of Vapour Plume Species and Deposition Residues Resulting from Pulsed Laser Ablation of a Graphite/Epoxy Composite

Abstract

A modified time-of-flight mass spectrometer fitted with a special collection stage for carbon-coated transmission electron microscope specimen grids is used to monitor laser-pulse ablation products from graphite/epoxy composite targets. Scanning electron microscopy observations show ablation damage to consist of matrix pyrolysis, fibre fracture and spallation of fragments which include elemental hydrogen, carbon epoxide and acetylene groups. Transmission electron microscope examination of specimen grids showed a variety of crystals and polycrystalline hexagonal graphites having a wide range of shapes including spheres and faceted polyhedra and platelets, textured flake structures, microrosettes. These observations lend some credibility to a model for laser-shock and pyrolysis effects which create molecular plume fragments and deposition fragments of hexagonal graphite.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1995
Accession Number
ADA408676

Entities

People

  • C. J. Miglionico
  • C. Stein
  • K. A. Lincoln
  • L. E. Murr
  • R. E. Roybal

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Air Platforms
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Ablation
  • Acetylenes
  • Composite Materials
  • Electron Microscopes
  • Electron Microscopy
  • Epoxy Composites
  • Graphitic Materials
  • Mass Spectrometers
  • Materials
  • Materials Engineering
  • Materials Science
  • Microscopes
  • Microscopy
  • Pulsed Lasers
  • Pyrolysis
  • Scanning Electron Microscopy
  • Spectrometers

Fields of Study

  • Physics

Readers

  • Materials Science and Engineering.
  • Pulsed Power and Plasma Physics.
  • Reinforced Composite Materials

Technology Areas

  • Directed Energy
  • Directed Energy - Pulsed-Laser Deposition
  • Microelectronics
  • Microelectronics - Graphene