Shape Forming via Colloidal Isopressing: Reformulating a Commerical Silicon Nitride Slurry with a Commercial Silane

Abstract

Colloidal Isopressing is a new shape forming method that requires a pre-consolidated slurry with a flow stress much less than that of a commercial throwing clay (< 0.1 MPa), so that it can be injected into a rubber cavity and isopressed. It is shown that the desired interparticle pair potential can be achieved with a commercial silane for a commercial Si3N4 aqueous slurry (NT 154-X12) containing densification aids. Unlike previous work, this silane has a relatively short molecular length and unlike previous results, the addition of salt was not needed to shorten the molecule and achieve the rheological behavior after pre-consolidation. The results of this study also show that the transition from a fluid-like to elastic-like behavior after consolidation was related to the relative density achieved during the pre-consolidation step, which was dependent on the consolidation pressure.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 2003
Accession Number
ADA414748

Entities

People

  • F. F. Lange
  • Hannes Essmann
  • Ryan Bock
  • V. K. Pujari

Organizations

  • University of California, Santa Barbara

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Ceramic Materials
  • Engineering
  • Filter Paper
  • Filtration
  • Flow
  • Fluid Flow
  • Materials
  • Materials Science
  • Measurement
  • Molecules
  • Particle Size
  • Particles
  • Powders
  • Rheology
  • Shape
  • Transitions
  • Viscosity

Readers

  • Agricultural Chemistry/Soil Science
  • Polymer Science and Technology
  • Powder metallurgy of Titanium alloys.