On-Site Processing and Subsampling of Surface Soil Samples for the Analysis of Explosives

Abstract

The on-site implementation of a sampling and analysis plan for the determination of explosives residues exposed a large uncertainty in our ability to quickly obtain representative subsamples from either large (>500 g) composite and/or large discrete samples. To improve the representativeness of on-site analysis, a simple on-site processing (grinding and mixing) and subsampling protocol was evaluated. Surface samples from three firing range characterization activities were taken through a procedure where the bulk samples were air-dried, sieved (#10, 2 mm), ground with a portable hand-operated mill, mixed, and then subsamples using layered bedding technique. This approach reduces laboratory-subsampling variance for both sparsely vegetated and vegetated surface soils. Moreover, during a subsequent dynamic sampling and analysis effort, this protocol was success fill in ranking explosives residue concentrations associated with a specific military training activity.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 2003
Accession Number
ADA416817

Entities

People

  • Alan D. Hewitt
  • Marianne E. Walsh

Organizations

  • Engineer Research and Development Center

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemical Analysis
  • Chemistry
  • Composite Materials
  • Energetic Materials
  • Engineering
  • Environmental Protection
  • Explosives
  • High Explosives
  • Liquid Chromatography
  • Materials
  • Munitions
  • New Hampshire
  • Particle Size
  • Propellants
  • Test Methods
  • Training
  • Unexploded Ammunition

Readers

  • Agricultural Chemistry/Soil Science
  • Regression Analysis.