New Strategies for Designing Receptors and Preparing Ultra-Sensitive Chemically Selective Electrode Surfaces

Abstract

Our research efforts have been focused on the design and synthesis of macrocyclic complexes based on the 'Weak-Link Approach' and their applications for recognition and separation technologies. Several important research discoveries have been made over the course of the project. A more thorough understanding of the fundamental parameters that control the formation of macrocyclic receptors formed via the Weak-Link Approach has been developed. In addition, novel hemilabile ligands that have used to form a new class of macrocycles referred to as 'molecular tweezers' have been designed. These structures can recognize molecule based on size, shape and the ability to form tt-stacking interactions. Using the Weak-Link Approach we have also synthesized a stable Rh(II) species, a set of chiral macrocyclic receptors and a series of heterobimetallic macrocyclic structures. This provides us with a library of compounds to investigate in future sensing applications. In the area of signal transduction, we have developed several fluorescent systems that utilize a new class of highly fluorescent ligands and Fluorescence Resonance Energy Transfer (FRET). Their receptor and molecular sensing properties has been investigated.

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Document Details

Document Type
Technical Report
Publication Date
Aug 31, 2003
Accession Number
ADA418189

Entities

People

  • Chad Mirkin
  • Thomas B. Higgins

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Advanced Materials
  • Cell Physiological Processes
  • Chemical Detectors
  • Chemical Synthesis
  • Chemistry
  • Dielectric Gases
  • Energy Transfer
  • Fluorescence
  • Inorganic Chemistry
  • Materials Science
  • Materials Testing
  • Molecules
  • Organic Chemistry
  • Recognition
  • Self Assembled Monolayers
  • Small Molecules
  • Students

Fields of Study

  • Chemistry

Readers

  • Distributed Systems and Data Platform Development
  • Electrochemical Surface Science
  • Organic Chemistry